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AIST Announces Installation of Noiseless Superconducting Detector Array for Mass Spectrometry

June 16  --  Dr. Masataka Ohkubo, leader and his colleagues of the Super-Spectroscopy System Research Group (SSSRG), the Research Institute of Instrumentation Frontier (RIIF), the National Institute of Advanced Industrial Science and Technology (AIST), an independent administrative institution, have implemented the installation technology for multi-cable (involving 100 coaxial cables) leading fast pulse signals out of 0.3 K cryogenic environment to room temperature one, needed for the development of advanced mass spectrometers.

  • Superconducting detector has 100 % detection efficiency for whatever kind of particles, while the installation technology in the cryogenic environment at around 0.3 K (= - 272.7 C), which is indispensable for the operation, has not been available so far for a large scale array detector.
  • The installation of 100 coaxial cables for the array detector have been successfully installed in the cryogenic environment. The heat flow through the cables is held at 5.4 microW, and the temperature rise is less than 0.015 K.
  • The size of the superconducting detector array can be upgraded by a degree of magnitude in comparison to the existing system involving a dozen of devices. The new installation technology, which enables a high mass resolution, will open the way to the practical use of mass spectrometer of 100 % detection efficiency for particles from atoms to macromolecules such as protein.

The superconducting detectors have excellent performance of detecting soft X rays and giant macromolecules, which was not available with the conventional semiconductor-based detectors in the X-ray spectrometry and the mass spectrometry. However, the system requires a cryogenic environment of temperature as low as 0.3 K and as the effective area of a single superconducting detector is as small as hundreds of micro m at the largest, an array of 100 superconducting detectors is required for the practical application of mass spectrometer with 100 % particle detecting efficiency.

In order to use the 100 superconducting detectors, a fast communication technology to link up the 0.3 K cryogenic environment with the room temperature ambient is needed. However, heat flow through the cable has been too great to implement the system through the conventional technology.

In the present study, the heat flow has been suppressed to less than 5.4 microW by using 100 coaxial cables as thin as 0.33 mm diameter, and making conductor from lower heat conduction metal. The feasibility of installation has been verified through the measurement of thermal conductivity with the coaxial cable under the cryogenic environment.

On the basis of these results, the prospect has been opened for practical use of the time-of-flight mass spectrometer (TOF MS) with ultimate sensitivity and 100 % particle detection efficiency covering particles from atoms to macromolecules such as protein, irrespective of molecular weight and molecular species.

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